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KBS52-2 - Nosyl deprotection of KBS51 #195

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KlementineJBS opened this issue Apr 24, 2024 · 2 comments
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KBS52-2 - Nosyl deprotection of KBS51 #195

KlementineJBS opened this issue Apr 24, 2024 · 2 comments

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@KlementineJBS
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Link to HIRAC and master page #186

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@KlementineJBS
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24.04.24

Protocol as usual. 55 mg of KBS52-1 (mixture of materials), 0.3 mmol 2-mercaptoethanol (23 mg, 21 uL), 0.6 mmol K2CO3 (85 mg) and 2 mL DMF

Heated to 140 C from ~11 am.

@KlementineJBS
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LRMS of crude RM

KBS52-2 RM.d.zip
KBS52-2 RM.pdf

@KlementineJBS KlementineJBS mentioned this issue Aug 7, 2024
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Linear amines (open cyclam) with naphthalene pendant groups
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