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Sources of Data

Edwin Tse edited this page Mar 10, 2020 · 48 revisions

Resources

Molecules and How to Visualize Them

The Master List - the Google Sheet of all OSM Compounds (Can filter Series 4).
OSIRIS DataWarrior (general purpose open-source chemoinformatics software).
Sister sheet that explains column headings (i.e. assays used).
Visualisation of OSM molecules on Cheminfo. The data may be visualized with Vortex. The Series 4 SDF can be generated on Cheminfo - here is a downloadable version from May 2016.

Lab Notebooks

The principal Labtrove ELN
Ed Tse's Labarchives ELN Short URL: https://tinyurl.com/OSM-Ed-Tse
Jasper Tyler's Lab Notebook
Marat Korsik's Lab Notebook
David Smith's Lab Notebook
Joshua Maxwell's Lab Notebook
Chase Smith's Labarchives ELN
Mark Coster's group (Griffith Uni) ELN
Old document from CRO describing synthetic chemistry of some members of series

Biological Evaluations

2014 (Jun) GSK Single shot potencies and July analysis of the actives (all data on Wiki and in Master List, checked by MHT)

2014 Syngene Potency Received (Nov) and Sent (Sept) (all data on Wiki and in Master List, checked by MHT)

2014 hERG data (figure in terms of IC50 or pIC50) file mirror

2015 (Nov) Syngene Potency (all data on Wiki and in Master List, checked by MHT)

2016 (June) Syngene Potency (sent May 2016) (all data on Wiki and in Master List, checked by MHT)

Metabolic/Physchem Data from Monash

Dundee Feb 2018 - ELN link

Pfizer Jan 2018

Dundee Oct 2017

Dundee July 2017

Also Dundee Jan 2017 re-evaluation of Frontrunners

Syngene-Kirk Correlation Nov 2016

Syngene Nov 2016 Labtrove

Theses

Ed Tse's PhD Thesis - Open Source Malaria: Potent Triazolopyrazine-Based Antiplasmodium Agents that Probe an Important Mechanism of Action

Papers

First paper based on this series is being written up here. Relevant 2016 review from MMV. 2017 New developments in anti-malarial target candidate and product profiles.

There is also a place on the separate Talks-Meetings-Publicity wiki for other items such as talks given, meetings and articles about OSM.

How To Join In

The To Do List
How to involve yourself in OSM is described in the Landing Page under "Join the Team".

Document Archive

Initial briefing document on the series written for MMV and a PDF summary of pharmacokinetics and efficacy; largely folded into the page below. (A minor error in the briefing document referring to the amides has been clarified.)

PDF of the Compounds Originally Inherited from MMV including structures and potencies (http://malaria.ourexperiment.org/osdd_malaria_shared/8106/MMV_triazolopyrazine_data.html older version of this file])

Old Summary of Data on Amides in the Series

ELN post containing many of the raw Chemdraw and picture files for this wiki page - if you generate new pictures, add to the ELN page. This resource needs porting to Github.

Project Reports: Devon Scott and Eduvie Omene, University of Edinburgh, Tom MacDonald, The University of Sydney.

Online Meetings

Most recent online meeting (May 2016) relevant to this series. Recording.

Background

What is OSM Series 4?

Aims, Concerns and Current Interest in Series 4

Sources of Data

Structure-Activity Relationships

Modification of Core Triazolopyrazine

Modification of Pyrazine Substitution Pattern

Modification of the Triazole Substitution

Pyrazine Side Chain Modifications - Ethers

Pyrazine Side Chain Modifications - Amides

Pyrazine Side Chain Modifications - Reversed Amides

Pyrazine Side Chain Modifications - Others

Metabolites

Biological Data Currently not Incorporated into the Main Wiki Sections

Physicochemical/Metabolic Parameters

Physicochem/metabolism/PK

Metabolism ID

Aldehyde Oxidase Assay

Stages and Efficacy

Liver Stage

Gametocyte Stage

In Vivo Efficacy

Potency vs. Resistant Strains

Other Observations

Mechanism of Action, Activity and Toxicity

Mechanism of Action: Possible PfATP4 Activity Deduced from Parasite Ion Regulation Assays

hERG Activity

Toxicity

Synthetic Chemistry

Synthetic Design

Synthesis of the Ether-Linked Series

Synthesis of the Amide-Linked Series

Synthesis of the Reverse Amide- Linked Series

Synthesis of Benzylic Functionalised Ether-Linked Series

Alternative Routes to the Triazolopyrazine Core

Triazolopyrazine telesubstitution

Biofunctionalisation

Late Stage Functionalisation

Fluoroalkene Isostere

Spectroscopy

Chirality, Relevant and Desirable Compounds

Chirality/Stereogenic Centres in This Series

Other Sources of Compounds Relevant to this Series

Desirable Compounds Not Yet Synthesised

Other Evaluations

Evaluations vs Other Organisms

Strings

Strings for Google

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