Ferrocenylmethyl ester synthesis
TLC Conditions
40:60 EtOAc:hexane
vanillin or iodine, UV
H NMR, 300 MHz, CDCl3
Peaks: 3.74 (s, 3H), 4.14 (s, 5H), 4.33 (s, 2H), 4.74 (s, 2H)
ESI LRMS m/z: 244.03 [M+H], 267.03 [M+Na]
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TLC Conditions
40:60 EtOAc:hexane
vanillin or iodine, UV
H NMR, 300 MHz, CDCl3
Peaks: 3.74 (s, 3H), 4.14 (s, 5H), 4.33 (s, 2H), 4.74 (s, 2H)
ESI LRMS m/z: 244.03 [M+H], 267.03 [M+Na]